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Top 4 Important considerations in the CO2 extraction process

Supercritical CO2 fluid extraction has the characteristics of fast mass transfer rate, strong penetrating ability, high extraction efficiency, and low operating temperature, and has become one of the most effective methods to obtain high-quality products.

What is a supercritical CO2 extraction machine?

The supercritical CO2 fluid extraction equipment is used for supercritical CO2 extraction. The supercritical fluid extraction machine is mainly composed of a freezing part, a pressurizing part, an extraction part, a separation part, and a recovery part, but according to the different production processes and fluid media, The configuration of the device is also different.

Read More: Supercritical CO2 Fluid

Work principle

supercritical CO2 extraction machine
Supercritical CO2 Extraction Machine

The main extraction process of the CO2 extraction machine consists of two parts: CO2 extraction and separation vessels.

In the CO2 extraction machine, at a specific temperature and pressure, the raw material is brought into contact with the supercritical CO2 fluid, and when the dynamic balance of the material components between the gas and liquid is reached, the temperature and pressure are adjusted to separate the extraction product from the supercritical CO2 fluid. Complete the whole process of supercritical extraction.

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1000L CO2 Extraction Machine

Supercritical CO2 extraction technology has been successfully used in medicine, food, chemical, and other industries, but in the production process, the following problems should be prevented:

Four important considerations

Important considerations 1#: Temperature monitoring

To prevent the temperature control instrument temperature control operation stable time is too long, and the fluctuation range is large. Since the temperature-measuring thermocouple sensor on the temperature controller is installed on the upper part of the CO2 extraction vessel and the CO2 extraction separator vessels, it is greatly affected by the ambient temperature.
In practical applications, the sensor should be directly inserted into the hot water tank, so as to solve this problem well.

Read More: CO2 Extraction Vessels

Important considerations 2#: “Water Blocking” Phenomenon During CO2 Extraction

The whole process of the supercritical CO2 extraction process

There is a “water block” phenomenon. In the application of supercritical CO2 extraction, since there is more or less water in the raw material, the CO2 in the separator after extraction usually carries a part of the water, and the CO2 containing a part of the water will freeze into ice when it is refrigerated and liquefied, causing the pipeline to block.

This phenomenon is called the “water blocking” phenomenon, also known as the “ice blocking” phenomenon.

Before the circulating CO2 gas enters the refrigerator, a dehydrator is set in the process flow, and a dehydrating agent such as silica gel or anhydrous CaCl2 is added to the dehydrator. It can also be transformed on the basis of the original purifier, and the purifier can be transformed into two parts, the upper part is a desiccant such as silica gel or anhydrous CaC2, and the lower part is a packing made of dense stainless steel, with a small hole in the middle. Stainless steel plates are separated.

Important considerations 3#: Blockage of CO2 extraction pipeline

The solid material in the extraction kettle should not be too fine. In the CO2 extraction process, the solid material is too fine to be carried out of the material basket by CO2 fluid, causing the blockage of the pipeline and reducing the mass transfer rate. The solution is to add loose and uniform stainless steel fillers in the extraction kettle to reduce the diffusion resistance of the material layer, thereby increasing the mass transfer rate, and effectively avoiding the channeling phenomenon (that is, the route with low CO2 fluid resistance passes through the material layer. , forming many pinholes, resulting in significantly uneven extraction).

Important considerations 4#: CO2 fractionation

Supercritical CO2 extraction and CO2 fractionation technology are combined. Because the CO2 fractionation tower is high and the pipe diameter of the segmented circulating heating water introduced into the fractionation tower is long, it is necessary to add thermal insulation materials outside.

Read More: CO2 Extraction Pumps